(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

Base Information

Chemical Name:(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate
CAS No.:1198356-04-5
Molecular Formula:C₁₈H₂₇BO₄
Molecular Weight:318.221
Hs Code.:

Synonyms:(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

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Technology Process of (S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

There total 7 articles about (S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: isopropyl (Z)-3-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-acrylate

: 1198356-04-5
(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; ZhaoPhos; hydrogen; In dichloromethane; at 30 ℃; for 6h; under 38002.6 Torr; enantioselective reaction; Autoclave;
DOI:10.1002/adsc.201900161

Reference yield: 78.0%

: 60512-85-8
(E)-isopropyl cinnamate

: 73183-34-3
bis(pinacol)diborane

: 1198356-04-5
(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

Guidance literature:: With C₂₄H₃₅N₂O₇Rh; sodium t-butanolate; In toluene; at 80 ℃; for 0.5h; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.086

Reference yield:

: 60512-85-8
(E)-isopropyl cinnamate

: 73183-34-3
bis(pinacol)diborane

: (R)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

: 1198356-04-5
(S)-isopropyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-phenylpropanoate

Guidance literature:: With Rh(Phebox-bn); sodium t-butanolate; In toluene; at 80 ℃; for 0.5h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/b915759j