(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

Base Information

Chemical Name:(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid
CAS No.:193679-43-5
Molecular Formula:C₁₃H₁₆O₆
Molecular Weight:268.266
Hs Code.:

Synonyms:(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

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Chemical Property of (3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

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Technology Process of (3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

There total 3 articles about (3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 193679-28-6
(E)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonyl-3-butenoic acid

: 193679-43-5
(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

: (3R)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (4R,5R)-(-)-MOD-DIOP; hydrogen; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo9710994

Reference yield:

: 621-59-0
isovanillin

: 193679-43-5
(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / sodium methoxide / methanol / 6 h / Heating

2: hydrogen / chlororhodium(I) (4R,5R)-MOD-DIOP complex / tetrahydrofuran; methanol / 7 h / 20 °C

With hydrogen; sodium methylate; chlororhodium(I) (4R,5R)-MOD-DIOP; In tetrahydrofuran; methanol; 1: Condensation / 2: Catalytic hydrogenation;
DOI:10.1021/jo990905z

Reference yield:

: 106-65-0
Dimethyl succinate

: 193679-43-5
(3S)-4-(3-hydroxy-4-methoxyphenyl)-3-methoxycarbonylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / sodium methoxide / methanol / 6 h / Heating

2: hydrogen / chlororhodium(I) (4R,5R)-MOD-DIOP complex / tetrahydrofuran; methanol / 7 h / 20 °C

With hydrogen; sodium methylate; chlororhodium(I) (4R,5R)-MOD-DIOP; In tetrahydrofuran; methanol; 1: Condensation / 2: Catalytic hydrogenation;
DOI:10.1021/jo990905z