(2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

Base Information

Chemical Name:(2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine
CAS No.:1032325-93-1
Molecular Formula:C₄₆H₅₅NO₄SSi₂
Molecular Weight:774.184
Hs Code.:

Synonyms:(2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

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Chemical Property of (2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

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Technology Process of (2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

There total 1 articles about (2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1032325-90-8
(2S,3R,4R,5R)-2-[(S)-1-hydroxybut-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidin-3-ol

: 100-39-0
benzyl bromide

: 1032325-93-1
(2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1002/chem.200701776

Reference yield:

: 1032325-93-1
(2S,3R,4R,5R)-3-(benzyloxy)-2-[(S)-1-(benzyloxy)but-3-enyl]-4-[dimethyl(phenyl)silyl]-5-{[dimethyl(phenyl)silyl]methyl}-1-tosylpyrrolidine

: C₄₅H₅₃NO₅SSi₂

Guidance literature:: With pyridine; sodium periodate; osmium(VIII) oxide; In water; acetonitrile; at 20 ℃; for 3h;
DOI:10.1002/chem.200701776