N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

Base Information

Chemical Name:N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide
CAS No.:960398-68-9
Molecular Formula:C₂₅H₃₇N₃O₃
Molecular Weight:427.587
Hs Code.:

Synonyms:N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

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Chemical Property of N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

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Technology Process of N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

There total 4 articles about N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 960398-67-8
benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

: 960398-68-9
N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; under 760.051 Torr;

Reference yield:

: 960398-87-2
C₁₇H₁₈N₄O₃

: 960398-68-9
N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 3.5 h / 20 °C / 2585.81 Torr

2.1: methanol / 2.5 h / 20 °C

2.2: 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C / 760.05 Torr

With hydrogen; palladium 10% on activated carbon; In methanol; ethanol; ethyl acetate;

Reference yield:

: 960398-80-5
benzyl 4-(4-(4-hydroxypentyl)phenyl)butylcarbamate

: 960398-68-9
N-(5-((1R)-2-(5-(4-(4-aminobutyl)phenyl)pentan-2-ylamino)-1-hydroxyethyl)-2-hydroxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 A molecular sieve; pyridinium chlorochromate / dichloromethane / 6 h / 20 °C

2.1: methanol / 2.5 h / 20 °C

2.2: 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C / 760.05 Torr

With 4 A molecular sieve; hydrogen; pyridinium chlorochromate; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane;