benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

Base Information

Chemical Name:benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate
CAS No.:960398-67-8
Molecular Formula:C₃₃H₄₃N₃O₅
Molecular Weight:561.722
Hs Code.:

Synonyms:benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

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Chemical Property of benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

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Technology Process of benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

There total 3 articles about benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 960398-66-7
(R)-N-(5-(2-amino-1-hydroxyethyl)-2-(benzyloxy)phenyl)acetamide

: 960398-51-0
benzyl 4-(4-(4-oxopentyl)phenyl)butylcarbamate

: 960398-67-8
benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

Guidance literature:: (R)-N-(5-(2-amino-1-hydroxyethyl)-2-(benzyloxy)phenyl)acetamide; benzyl 4-(4-(4-oxopentyl)phenyl)butylcarbamate; In methanol; at 20 ℃; for 2.5h;

With sodium cyanoborohydride; In methanol; at 20 ℃;

Reference yield:

: 960398-87-2
C₁₇H₁₈N₄O₃

: 960398-67-8
benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 3.5 h / 20 °C / 2585.81 Torr

2.1: methanol / 2.5 h / 20 °C

2.2: 20 °C

With hydrogen; palladium 10% on activated carbon; In methanol; ethanol; ethyl acetate;

Reference yield:

: 960398-80-5
benzyl 4-(4-(4-hydroxypentyl)phenyl)butylcarbamate

: 960398-67-8
benzyl (4-(4-(4-(R)-2-((3-acetamido-4-benzyloxy)phenyl)-2-hydroxyethylamino)pentyl)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4 A molecular sieve; pyridinium chlorochromate / dichloromethane / 6 h / 20 °C

2.1: methanol / 2.5 h / 20 °C

2.2: 20 °C

With 4 A molecular sieve; pyridinium chlorochromate; In methanol; dichloromethane;