Technology Process of 2-(2,4-dinitrobenzamido)-1,2-diphenylethyl benzoate
There total 7 articles about 2-(2,4-dinitrobenzamido)-1,2-diphenylethyl benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate;
In
chloroform;
at 20 ℃;
enantioselective reaction;
DOI:10.1002/anie.201400169
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide; ammonium chloride / methanol; water / 12 h / 60 °C
2: triphenylphosphine / acetonitrile / 12 h / 60 °C / Inert atmosphere
3: triethylamine / tetrahydrofuran / 1.5 h / -40 - -10 °C
4: (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / chloroform / 20 °C
With
sodium azide; (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; ammonium chloride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; chloroform; water; acetonitrile;
DOI:10.1002/anie.201400169
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine / acetonitrile / 12 h / 60 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 1.5 h / -40 - -10 °C
3: (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / chloroform / 20 °C
With
(S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1002/anie.201400169
