(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

Base Information

Chemical Name:(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran
CAS No.:116612-17-0
Molecular Formula:C₂₅H₃₆O₇
Molecular Weight:448.557
Hs Code.:

Synonyms:(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

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Chemical Property of (2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

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Technology Process of (2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

There total 7 articles about (2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116640-23-4
(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-2,3-(isopropylidenedioxy)-5-<(1R)-1,2-(isopropylidenedioxy)ethyl>-4-methyltetrahydrofuran

: 116612-17-0
(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent CH₃COOH / H₂O

2: 4-DMAP, pyridine

With pyridine; dmap; acetic acid; In water;
DOI:10.1016/S0040-4039(00)80175-6

Reference yield:

: 103516-20-7
3-deoxy-1,2:5,6-di-O-isopropylidene-3-C-methyl-3-C-vinyl-α-D-allofuranose

: 116612-17-0
(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

Guidance literature:: Multi-step reaction with 6 steps

2: 90 percent / benzene / Heating

3: DIBAL-H / CH₂Cl₂ / -40 °C

5: 50percent CH₃COOH / H₂O

6: 4-DMAP, pyridine

With pyridine; dmap; diisobutylaluminium hydride; acetic acid; In dichloromethane; water; benzene;
DOI:10.1016/S0040-4039(00)80175-6

Reference yield:

: 116612-14-7
(3aR,5S,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2,6-trimethyl-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbaldehyde

: 116612-17-0
(2R,3R,4R,5S)-4-<(E)-3-(benzyloxy)-1-propenyl>-5-<(1R)-<1-hydroxy-2-(2,2-dimethylpropionyl)oxy>ethyl>-2,3-(isopropylidenedioxy)-4-methyltetrahydrofuran

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / benzene / Heating

2: DIBAL-H / CH₂Cl₂ / -40 °C

4: 50percent CH₃COOH / H₂O

5: 4-DMAP, pyridine

With pyridine; dmap; diisobutylaluminium hydride; acetic acid; In dichloromethane; water; benzene;
DOI:10.1016/S0040-4039(00)80175-6