Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

Base Information

Chemical Name:Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate
CAS No.:1325717-68-7
Molecular Formula:C₁₄H₁₄ClNO₅
Molecular Weight:311.722
Hs Code.:

Synonyms:Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

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Chemical Property of Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

Chemical Property:

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Technology Process of Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

There total 5 articles about Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1325717-58-5
2-(4-Chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 1325717-68-7
Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

Guidance literature:: In methanol; hexane; toluene; at 20 ℃; for 0.166667h;

Reference yield:

: 1325717-56-3
2-(4-Chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carbaldehyde

: 1325717-68-7
Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; silver nitrate / 1,4-dioxane; water / 3 h / 20 °C

2: toluene; hexane; methanol / 0.17 h / 20 °C

With silver nitrate; sodium hydroxide; In 1,4-dioxane; methanol; hexane; water; toluene;

Reference yield:

: 22091-36-7
4-chloromethyl-2-(4-chlorophenyl)oxazole

: 1325717-68-7
Methyl 2-(4-chlorophenyl)-4-[(methoxymethoxy)methyl]-1,3-oxazole-5-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 2 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1.17 h / 0 - 20 °C

2.2: 2.16 h / 0 - 20 °C

3.1: n-butyllithium / hexane; diethyl ether / 1 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: sodium hydroxide; silver nitrate / 1,4-dioxane; water / 3 h / 20 °C

5.1: toluene; hexane; methanol / 0.17 h / 20 °C

With n-butyllithium; sodium hydride; silver nitrate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; hexane; water; toluene; mineral oil;