C.I. Basic Blue 3

Base Information

Chemical Name:C.I. Basic Blue 3
CAS No.:33203-82-6
Deprecated CAS:127302-45-8,6703-67-9,77641-00-0,940888-75-5,2097526-91-3
Molecular Formula:C₂₀H₂₆N₃O*Cl
Molecular Weight:359.899
Hs Code.:
European Community (EC) Number:251-403-5,611-321-6,614-016-6
NSC Number:409100,367084
UNII:H82L80329Y
DSSTox Substance ID:DTXSID30873926
Wikidata:Q27279744
ChEMBL ID:CHEMBL389921
Mol file:33203-82-6.mol

Synonyms:Basic Blue 3;BB 3 dye;C.I. 51004 Basic Blue 3;C.I. Basic Blue 3

Suppliers and Price of C.I. Basic Blue 3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Basic Blue 3
10g
$ 45.00

Sigma-Aldrich
Basic Blue 3 Dye content 25 %
100g
$ 107.00

Chem-Impex
BasicBlue3,≥25%(Dyecontent),suitableforHematology&Histology ≥25%(Dyecontent)
100G
$ 111.82

American Custom Chemicals Corporation
BASIC BLUE 3 95.00%
5MG
$ 501.70

Total 35 raw suppliers

Chemical Property of C.I. Basic Blue 3

Chemical Property:

Vapor Pressure:3.24E-09mmHg at 25°C
Melting Point:205 °C (dec.)(lit.)
Refractive Index:1.575
Boiling Point:475.7°C at 760 mmHg
Flash Point:241.5°C
PSA：32.51000
Density:1.09g/cm³
LogP:1.95850
Storage Temp.:room temp
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:359.1764402
Heavy Atom Count:25
Complexity:533

Purity/Quality:

99% ^*data from raw suppliers

Basic Blue 3 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CCN(CC)C1=CC2=C(C=C1)N=C3C=CC(=[N+](CC)CC)C=C3O2.[Cl-]
Uses Basic blue 3 has a brilliant blue shade and thus has been used as a colorant in dyeing acrylic fabrics.

Technology Process of C.I. Basic Blue 3

There total 5 articles about C.I. Basic Blue 3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: N,N-diethyl-3-methoxy-4-nitrosoaniline

: 91-68-9
3-diethylaminophenol

: 33203-82-6,55840-82-9
basic blue 3

Guidance literature:: With hydrogenchloride; In isopropyl alcohol; at 70 - 100 ℃; for 12h; Inert atmosphere;
DOI:10.1039/d0cc05133k

Reference yield:

: C₁₁H₁₆N₂O₂*HCl

: 91-68-9
3-diethylaminophenol

: 33203-82-6,55840-82-9
basic blue 3

Guidance literature:: In isopropyl alcohol; at 20 ℃; for 4h;
DOI:10.1021/jm070201e

Reference yield:

: 91-68-9
3-diethylaminophenol

: 33203-82-6,55840-82-9
basic blue 3

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / acetonitrile / 1 h

1.2: 70 °C

2.1: hydrogenchloride; sodium nitrite / water / 2 h / Cooling with ice

2.2: pH 9

3.1: hydrogenchloride / isopropyl alcohol / 12 h / 70 - 100 °C / Inert atmosphere

With hydrogenchloride; sodium hydroxide; sodium nitrite; In water; isopropyl alcohol; acetonitrile;
DOI:10.1039/d0cc05133k