C₁₃H₁₄FNO₂

Base Information

Chemical Name:C₁₃H₁₄FNO₂
CAS No.:1186046-95-6
Molecular Formula:C₁₃H₁₄FNO₂
Molecular Weight:235.258
Hs Code.:

C<sub>13</sub>H<sub>14</sub>FNO<sub>2</sub>

Synonyms:C₁₃H₁₄FNO₂

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Chemical Property of C₁₃H₁₄FNO₂

Chemical Property:

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Technology Process of C₁₃H₁₄FNO₂

There total 6 articles about C₁₃H₁₄FNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186046-94-5
C₁₃H₁₆FNO₂

: 1186046-95-6
C₁₃H₁₄FNO₂

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 403-40-7
1-(4-fluorophenyl)ethylamine

: 1186046-95-6
C₁₃H₁₄FNO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / Cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 60 °C

3.1: tert.-butyl lithium / tetrahydrofuran / 0.25 h / -78 °C

3.2: 0.33 h / -78 °C

4.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

With pyridine; tert.-butyl lithium; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1119-46-6
5-chloro-valeric acid

: 1186046-95-6
C₁₃H₁₄FNO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 60 °C

3.1: tert.-butyl lithium / tetrahydrofuran / 0.25 h / -78 °C

3.2: 0.33 h / -78 °C

4.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

With tert.-butyl lithium; sodium hydride; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;