C₁₁H₁₂N₂S

Base Information

Chemical Name:C₁₁H₁₂N₂S
CAS No.:21331-38-4
Molecular Formula:C₁₁H₁₂N₂S
Molecular Weight:204.296
Hs Code.:

C<sub>11</sub>H<sub>12</sub>N<sub>2</sub>S

Synonyms:C₁₁H₁₂N₂S

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Chemical Property of C₁₁H₁₂N₂S

Chemical Property:

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Technology Process of C₁₁H₁₂N₂S

There total 4 articles about C₁₁H₁₂N₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 598-52-7
1-(methyl)-thiourea

: 1794-48-5
1-bromo-3-phenylprop-2-yne

: 21331-38-4
C₁₁H₁₂N₂S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1055/s-0029-1217700

Reference yield:

: 591-50-4
iodobenzene

: 21331-38-4
C₁₁H₁₂N₂S

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide

2: triethylamine / dichloromethane

3: lithium bromide / tetrahydrofuran; dichloromethane

4: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 130 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1055/s-0029-1217700

Reference yield:

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 21331-38-4
C₁₁H₁₂N₂S

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane

2: lithium bromide / tetrahydrofuran; dichloromethane

3: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 130 °C / Microwave irradiation

With potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0029-1217700