Technology Process of Atreleuton
There total 5 articles about Atreleuton which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dichloro bis(acetonitrile) palladium(II); copper(l) iodide; diethylamine; triphenylphosphine;
In
N,N-dimethyl-formamide;
for 22h;
Ambient temperature;
DOI:10.1021/jm00024a004
- Guidance literature:
-
With
hydrogenchloride; sodium hydroxide; triethylamine;
In
methanol; n-heptane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-butyllithium, 2.) tetrakis(triphenylphosphine)palladium(0) / 1.) ether, THF, hexane, 0 deg C, 1.5 h, 2.) ether, hexane, THF, RT, overnight
2: 95 percent / N-iodosuccinimide, acetic acid / CHCl3 / 1 h / Ambient temperature
3: 18 percent / triphenylphosphine, bis(acetonitrile)palladium(II) chloride, copper(I) iodide, diethylamine / dimethylformamide / 22 h / Ambient temperature
With
dichloro bis(acetonitrile) palladium(II); N-iodo-succinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; acetic acid; diethylamine; triphenylphosphine;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00024a004