3,3',4,4'-Tetraaminodiphenyl ether

Base Information

Chemical Name:3,3',4,4'-Tetraaminodiphenyl ether
CAS No.:2676-59-7
Molecular Formula:C12H14 N4 O
Molecular Weight:230.269
Hs Code.:
European Community (EC) Number:220-226-5
UNII:A8NR6PP85T
DSSTox Substance ID:DTXSID90181271
Nikkaji Number:J192.189D
Wikidata:Q83051880
ChEMBL ID:CHEMBL1448416
Mol file:2676-59-7.mol

Synonyms:3,3',4,4'-tetraaminodiphenyl ether;3,3',4,4'-tetraaminodiphenyl ether tetrahydrochloride

Suppliers and Price of 3,3',4,4'-Tetraaminodiphenyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
4-(3,4-Diaminophenoxy)-1,2-benzenediamine
10g
$ 1170.00

Matrix Scientific
4-(3,4-Diaminophenoxy)-1,2-benzenediamine
5g
$ 810.00

Matrix Scientific
4-(3,4-Diaminophenoxy)-1,2-benzenediamine
1g
$ 316.00

Aronis compounds
4,4'-oxydi(1,2-benzenediamine)
10mg
$ 20.00

Aronis compounds
4,4'-oxydi(1,2-benzenediamine)
1mg
$ 12.00

American Custom Chemicals Corporation
4-(3,4-DIAMINOPHENOXY)BENZENE-1,2-DIAMINE 95.00%
5MG
$ 935.00

AK Scientific
3,3',4,4'-Tetraaminodiphenylether
10g
$ 1629.00

Total 13 raw suppliers

Chemical Property of 3,3',4,4'-Tetraaminodiphenyl ether

Chemical Property:

Melting Point:147-150 °C
Boiling Point:477.3°Cat760mmHg
PKA:5.09±0.10(Predicted)
Flash Point:278.5°C
PSA：113.31000
Density:1.361g/cm³
LogP:4.13250
XLogP3:0.7
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:230.11676108
Heavy Atom Count:17
Complexity:227

Purity/Quality:

99% ^*data from raw suppliers

4-(3,4-Diaminophenoxy)-1,2-benzenediamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1OC2=CC(=C(C=C2)N)N)N)N

Technology Process of 3,3',4,4'-Tetraaminodiphenyl ether

There total 14 articles about 3,3',4,4'-Tetraaminodiphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3273-78-7
4-(4-amino-3-nitrophenoxy)-2-nitrophenylamine

: 2676-59-7
bis(3,4-diaminophenyl)ether

Guidance literature:: With 10% Pd/C; hydrogen; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2012.06.102

Reference yield:

: 2676-59-7
bis(3,4-diaminophenyl)ether

Guidance literature:: 3.3'-Dinitro-4.4'-Diaminodiphenylether, Pt+Pd/Al2O3, org. Lsgm., NH3, 20grad-100grad, 1atm-100atm (Hydrier.);

Reference yield:

: 101-63-3
bis(4-nitrophenyl)ether

: 2676-59-7
bis(3,4-diaminophenyl)ether

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NH₂NH₂; FeCl₃; activated charcoal / dioxane

2: 93 percent / chlorobenzene / 2 h / 90 - 95 °C

3: 94 percent / HNO₃; AcOH; Ac₂O / urea / 50 - 60 °C

4: 96 percent / aq. NaOH / propan-2-ol / 80 °C

5: 60 percent / NH₂NH₂; FeCl₃; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C

With sodium hydroxide; nitric acid; acetic anhydride; iron(III) chloride; pyrographite; acetic acid; hydrazine; urea; In 1,4-dioxane; chlorobenzene; isopropyl alcohol; butan-1-ol;
DOI:10.1007/s11176-005-0459-8