4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide

Base Information

• Chemical Name: 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide
• CAS No.: 1458054-79-9
• Molecular Formula: C₂₇H₃₃N₅O₆S
• Molecular Weight: 555.655

Synonyms:4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide

Chemical Property of 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide

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Technology Process of 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide

There total 1 articles about 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

4-[(4-azidophenyl)sulfonyl]-N-(tetrahydro-2H-pyran-2-yloxy)-tetrahydro-2H-pyran-4-carboxamide (1314020-65-9) + 4-ethynyl-N,N-dimethylaniline (17573-94-3,752235-18-0) → 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide (1458054-79-9)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; Inert atmosphere;

DOI:10.1039/c3ob41046c

Reference yield: 94.0%

4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenyl)sulfonyl)-N-((tetrahydro-2H-pyran-2-yl)oxy)tetrahydro-2H-pyran-4-carboxamide (1458054-79-9) → 4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-phenyl)sulfonyl)-N-hydroxytetrahydro-2H-pyran-4-carboxamide hydrochloride (1458054-42-6)

Guidance literature:

With hydrogenchloride; methanol; In 1,4-dioxane; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1039/c3ob41046c

upstream raw materials:

4-[(4-azidophenyl)sulfonyl]-N-(tetrahydro-2H-pyran-2-yloxy)-tetrahydro-2H-pyran-4-carboxamide

4-ethynyl-N,N-dimethylaniline

Downstream raw materials:

4-((4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-phenyl)sulfonyl)-N-hydroxytetrahydro-2H-pyran-4-carboxamide hydrochloride

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