1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

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Chemical Name:1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione
CAS No.:256932-99-7
Molecular Formula:C₄₀H₃₇NO₅S₄
Molecular Weight:740.001
Hs Code.:

1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1<i>H</i>-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

Synonyms:1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

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Chemical Property of 1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

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Technology Process of 1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

There total 5 articles about 1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 13196-35-5
3-(dimethylamino)-1-(thiophen-2-yl)propan-1-one

: 256932-97-5
C₂₆H₂₅NO₃S₂

: 256932-99-7
1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

Guidance literature:: With sodium cyanide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)01904-8

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 256932-99-7
1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: NaCN / dimethylformamide

2: AcOH / toluene / 32 °C

4: 45 percent / NaCN / dimethylformamide

With sodium cyanide; acetic acid; In N,N-dimethyl-formamide; toluene; 1: Stetter reaction / 2: Condensation / 3: Formylation / 4: Stetter reaction;
DOI:10.1016/S0040-4039(99)01904-8

Reference yield:

: 13196-35-5
3-(dimethylamino)-1-(thiophen-2-yl)propan-1-one

: 256932-99-7
1-(5-{1-(4-hexyloxy-phenyl)-5-[5-(4-oxo-4-thiophen-2-yl-butyryl)-thiophen-2-yl]-1H-pyrrol-2-yl}-thiophen-2-yl)-4-thiophen-2-yl-butane-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: NaCN / dimethylformamide

2: AcOH / toluene / 32 °C

4: 45 percent / NaCN / dimethylformamide

With sodium cyanide; acetic acid; In N,N-dimethyl-formamide; toluene; 1: Stetter reaction / 2: Condensation / 3: Formylation / 4: Stetter reaction;
DOI:10.1016/S0040-4039(99)01904-8