2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine
CAS No.:488827-75-4
Molecular Formula:C₃₆H₃₇NO₁₄S
Molecular Weight:739.754
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

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Chemical Property of 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

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Technology Process of 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

There total 1 articles about 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 124-63-0
methanesulfonyl chloride

: 144310-56-5
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranosylamine

: 488827-75-4
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1016/S0957-4166(02)00377-4

Reference yield: 80.0%

: 488827-75-4
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

: 225662-83-9
1,6-anhydro-2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranosylamine

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; at 40 ℃; for 0.25h; under 20 Torr;
DOI:10.1016/S0957-4166(02)00377-4

Reference yield:

: 488827-75-4
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-mesyl-β-D-glucopyranosylamine

: 3S,4R,6R-3,4,5-tribenzoyloxy-6-hydroxyazepan

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / hexamethylphosphoric acid triamide

2: Cl₂ / CH₂Cl₂

3: 98 percent / NaCNBH₃ / methanol

With sodium methylate; chlorine; sodium cyanoborohydride; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; 1: Cyclization / 2: N-deprotection / 3: Reduction;
DOI:10.1016/S0040-4039(99)00649-8