3,4-Dimethoxybenzaldehyde benzylphenylhydrazone

Base Information

Chemical Name:3,4-Dimethoxybenzaldehyde benzylphenylhydrazone
CAS No.:80165-60-2
Molecular Formula:C₂₂H₂₂N₂O₂
Molecular Weight:346.429
Hs Code.:
European Community (EC) Number:661-420-3

Synonyms:AKOS024339108;3,4-DIMETHOXYBENZALDEHYDE BENZYLPHENYLHYDRAZONE

Suppliers and Price of 3,4-Dimethoxybenzaldehyde benzylphenylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3,4-Dimethoxybenzaldehyde benzylphenylhydrazone

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:346.168127949
Heavy Atom Count:26
Complexity:416

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C=NN(CC2=CC=CC=C2)C3=CC=CC=C3)OC
Isomeric SMILES:COC1=C(C=C(C=C1)/C=N/N(CC2=CC=CC=C2)C3=CC=CC=C3)OC

Technology Process of 3,4-Dimethoxybenzaldehyde benzylphenylhydrazone

There total 3 articles about 3,4-Dimethoxybenzaldehyde benzylphenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 55754-32-0
N-(3,4-dimethoxybenzylidene)phenylhydrazine

: 100-39-0
benzyl bromide

: 80165-60-2
2-(3,4-dimethoxybenzylidene)-1-benzyl-1-phenylhydrazine

Guidance literature:: N-(3,4-dimethoxybenzylidene)phenylhydrazine; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo2005632

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 80165-60-2
2-(3,4-dimethoxybenzylidene)-1-benzyl-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / ethanol; water / 20 - 80 °C

2.1: sodium hydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With sodium acetate; sodium hydride; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo2005632

Reference yield:

: 62-53-3
aniline

: 80165-60-2
2-(3,4-dimethoxybenzylidene)-1-benzyl-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: sodium acetate / ethanol; water / 20 - 80 °C

3.1: sodium hydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.2: 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium acetate; sodium hydride; sodium nitrite; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo2005632