(η(3)-allyl)PdCl * tricyclohexylphosphine

Base Information

Chemical Name:(η(3)-allyl)PdCl * tricyclohexylphosphine
CAS No.:125893-61-0
Molecular Formula:C₂₁H₃₈ClPPd
Molecular Weight:463.379
Hs Code.:

Synonyms:(η(3)-allyl)PdCl * tricyclohexylphosphine

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Chemical Property of (η(3)-allyl)PdCl * tricyclohexylphosphine

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Technology Process of (η(3)-allyl)PdCl * tricyclohexylphosphine

There total 3 articles about (η(3)-allyl)PdCl * tricyclohexylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 2622-14-2
tricyclohexylphosphine

: 125893-61-0
(η(3)-allyl)PdCl * tricyclohexylphosphine

Guidance literature:: In tetrahydrofuran; (N2); THF was added via syringe to mixt. of Pd compd. and P ligand in Schlenk flask; soln. was stirred at room temp. for 1 h; evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om0306224

Reference yield:

: 845547-55-9
[((allyl)Pd(PCy3))2(μ-Cl)]PF6

: 2622-14-2
tricyclohexylphosphine

: 125893-61-0
(η(3)-allyl)PdCl * tricyclohexylphosphine

: 1009638-61-2
[(allyl)Pd(PCy₃)2]PF₆

Guidance literature:: In dichloromethane-d2; ⁽²⁾H₈-toluene; (N2); Schlenk technique; P ligand was added to soln. of Pd complex in toluene-d8/CD2Cl2 (2/1.5); NMR monitoring;
DOI:10.1021/om700921f