tricyclohexylphosphinepalladium allyl iodide

Base Information

• Chemical Name: tricyclohexylphosphinepalladium allyl iodide
• CAS No.: 244159-81-7
• Molecular Formula: C₂₁H₃₈IPPd
• Molecular Weight: 554.831
• Mol file: 244159-81-7.mol

Synonyms:

Chemical Property of tricyclohexylphosphinepalladium allyl iodide

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of tricyclohexylphosphinepalladium allyl iodide

There total 1 articles about tricyclohexylphosphinepalladium allyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(η(3)-allyl)PdCl * tricyclohexylphosphine (125893-61-0) + sodium iodide (7681-82-5,24359-64-6,41927-88-2,115813-40-6) → tricyclohexylphosphinepalladium allyl iodide (244159-81-7)

Guidance literature:

In dichloromethane; (Ar); std. Schlenk technique; Pd complex (1 equiv.) and NaI (10 equiv.) were suspnd. for 18 h; filtered through Celite; evapd.; triturated with hexane; elem. anal.;

DOI:10.1021/om8008052

upstream raw materials:

(η(3)-allyl)PdCl * tricyclohexylphosphine

sodium iodide