(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

Base Information

Chemical Name:(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate
CAS No.:1352145-60-8
Molecular Formula:C₂₄H₃₆O₆
Molecular Weight:420.546
Hs Code.:

Synonyms:(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

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Technology Process of (R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

There total 7 articles about (R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 504-85-8
4-methyl-pent-3-enoic acid

: 1352145-58-4
(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

: 1352145-60-8
(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ol203060v

Reference yield: 65.0%

: 504-85-8
4-methyl-pent-3-enoic acid

: 1352145-55-1
(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

: 1352145-60-8
(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol203060v

Reference yield:

: 1352145-56-2
C₁₈H₂₆O₅

: 1352145-60-8
(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; In tetrahydrofuran; methanol; 2: Mitsunobu reaction;
DOI:10.1021/ol203060v