(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

Base Information

Chemical Name:(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol
CAS No.:1352145-58-4
Molecular Formula:C₁₈H₂₈O₅
Molecular Weight:324.417
Hs Code.:

Synonyms:(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

Suppliers and Price of (R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

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Technology Process of (R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

There total 6 articles about (R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1352145-57-3
C₂₀H₃₀O₆

: 1352145-58-4
(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

Guidance literature:: With methanol; potassium carbonate; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol203060v

Reference yield: 45.0%

: 108-05-4,9003-20-7
vinyl acetate

: 1352145-55-1
(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

: 1352145-59-5
(S)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

: 1352145-58-4
(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

: 1352145-57-3
C₂₀H₃₀O₆

Guidance literature:: With Burkholderia cepacia lipase; In tert-butylmethyl ether; at 20 ℃; for 24h; optical yield given as %ee; Inert atmosphere; Resolution of racemate; Enzymatic reaction;
DOI:10.1021/ol203060v

Reference yield:

: 1352145-56-2
C₁₈H₂₆O₅

: 1352145-58-4
(R)-(E)-4-(2-(methoxymethoxy)-3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

2: Burkholderia cepacia lipase / tert-butylmethyl ether / 24 h / 20 °C / Inert atmosphere; Resolution of racemate; Enzymatic reaction

With Burkholderia cepacia lipase; sodium tetrahydroborate; In methanol; tert-butylmethyl ether;
DOI:10.1021/ol203060v