N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

Base Information

Chemical Name:N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea
CAS No.:244288-40-2
Molecular Formula:C₂₉H₃₃N₃O₂S
Molecular Weight:487.666
Hs Code.:

Synonyms:N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

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Chemical Property of N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

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Technology Process of N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

There total 3 articles about N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 313695-74-8
N-[(1S,2S)-2-amino-1,2-diphenylethyl]-N'-cyclohexylthiourea

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 244288-40-2
N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo000745n

Reference yield:

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 244288-40-2
N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / acetonitrile / 24 h / 20 °C

2: 85 percent / Et₃N / CH₂Cl₂ / 20 °C

With triethylamine; In dichloromethane; acetonitrile; 1: Substitution / 2: Acylation;
DOI:10.1021/jo000745n

Reference yield:

: 1122-82-3
isothiocyanatocyclohexane

: 244288-40-2
N-[(1S,2S)-2-benzyloxycarbonylamino-1,2-diphenylethyl]-N'-cyclohexylthiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / acetonitrile / 24 h / 20 °C

2: 85 percent / Et₃N / CH₂Cl₂ / 20 °C

With triethylamine; In dichloromethane; acetonitrile; 1: Substitution / 2: Acylation;
DOI:10.1021/jo000745n