C₁₄H₁₁ClN₂O₃

Base Information

• Chemical Name: C₁₄H₁₁ClN₂O₃
• CAS No.: 916990-27-7
• Molecular Formula: C₁₄H₁₁ClN₂O₃
• Molecular Weight: 290.706
• Mol file: 916990-27-7.mol

Synonyms:C₁₄H₁₁ClN₂O₃

Chemical Property of C₁₄H₁₁ClN₂O₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₁ClN₂O₃

There total 1 articles about C₁₄H₁₁ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C16H15ClN2O3 (916990-25-5) → C14H11ClN2O3 (916990-27-7)

Guidance literature:

C₁₆H₁₅ClN₂O₃; With lithium iodide; In pyridine; at 115 ℃; for 7.5h;

With hydrogenchloride; water;

Reference yield: 76.0%

1-(3-aminopropyl)piperidine (3529-08-6) + C14H11ClN2O3 (916990-27-7) → C22H27ClN4O2 (916990-29-9)

Guidance literature:

C₁₄H₁₁ClN₂O₃; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.0333333h;

1-(3-aminopropyl)piperidine; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield: 37.0%

C14H11ClN2O3 (916990-27-7) + tert-butyl alcohol (75-65-0) → C18H20ClN3O3 (916990-38-0)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; for 28h; Heating / reflux;

upstream raw materials:

C₁₆H₁₅ClN₂O₃

Downstream raw materials:

C₁₈H₂₀ClN₃O₃

C₂₂H₂₇ClN₄O₂

Refernces