chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

Base Information

Chemical Name:chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)
CAS No.:335377-52-1
Molecular Formula:C₃₄H₃₃ClP₃Pt*Cl₃Sn
Molecular Weight:990.159
Hs Code.:

Synonyms:chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

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Chemical Property of chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

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Technology Process of chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

There total 5 articles about chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 33847-49-3
[chloro(bis[(2-diphenylphosphino)ethyl]phenylphosphine)platinum(II)] chloride

: tin(ll) chloride

: 335377-52-1
chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

Guidance literature:: In methanol; dichloromethane; soln. of SnCl2 (0.25 mmol) in MeOH/CH2Cl2 (1/1) added to soln. of Pt complex (0.25 mmol) in CH2Cl2, stirred for 7 h; evapd. in vac., residue recrystd. (CH2Cl2/Et2O), dried. (vac.); elem. anal.;
DOI:10.1016/S0277-5387(01)00716-1

Reference yield:

: 69462-32-4
AuCl(S(CH₂CH₂OH)2)

: PtP(C₆H₅)3(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2⁽²⁺⁾*2SnCl₃^(1-)=PtP(C₆H₅)3(C₆H₅)2PCH₂CH₂PC₆H₅CH₂CH₂P(C₆H₅)2(SnCl₃)2

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: PtAu(bis(2-diphenylphosphinoethyl)phenylphosphine)Cl₃

: 335377-52-1
chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

Guidance literature:: In methanol; chloroform-d1; dichloromethane; Pt-complex in CDCl3 was reacted with Au-complex in MeOH and CH2Cl2, mixt. was stirred for 12 h, filtered off; monitored by NMR;
DOI:10.1016/S0020-1693(00)00329-7

Reference yield:

: 23582-02-7
bis(2-diphenylphosphinoethyl)phenylphosphine

: 335377-52-1
chloro(bis(2-diphenylphosphinoethyl)phenylphosphine)platinum(II) trichlorostannate(II)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: methanol; dichloromethane

In methanol; dichloromethane; benzene;
DOI:10.1016/S0277-5387(01)00716-1