C₃₂H₃₃N₅O₆

Base Information

Chemical Name:C₃₂H₃₃N₅O₆
CAS No.:1610517-71-9
Molecular Formula:C₃₂H₃₃N₅O₆
Molecular Weight:583.644
Hs Code.:

C<sub>32</sub>H<sub>33</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₃₂H₃₃N₅O₆

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Chemical Property of C₃₂H₃₃N₅O₆

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Technology Process of C₃₂H₃₃N₅O₆

There total 10 articles about C₃₂H₃₃N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.3%

: C₃₂H₃₄N₂O₆

: 1610517-71-9
C₃₂H₃₃N₅O₆

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 140 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.04.042

Reference yield: 85.3%

: C₃₂H₃₂N₂O₆

: 1610517-71-9
C₃₂H₃₃N₅O₆

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 140 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.04.042

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 1610517-71-9
C₃₂H₃₃N₅O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridine / 23 h / 20 - 70 °C

2.1: trifluoroacetic acid; water / dichloromethane / 1.25 h / 20 °C / Cooling with ice

3.1: Dess-Martin periodane / acetonitrile / 2 h / Reflux

4.1: 0 - 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 0 °C

5.2: 20 °C

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20.5 h / 0 - 20 °C

6.2: 5 h / 0 - 20 °C

7.1: palladium 10% on activated carbon; cyclohexene / methanol / 24 h / Reflux

8.1: pyridine / 3 h / 20 °C / Inert atmosphere; Cooling with ice

9.1: triphenylphosphine; di-isopropyl azodicarboxylate / acetonitrile / 0 - 20 °C / Inert atmosphere

10.1: sodium azide / N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

With pyridine; sodium azide; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; trifluoroacetic acid; cyclohexene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4.1: |Wittig Olefination / 9.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2014.04.042