(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

Base Information

Chemical Name:(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde
CAS No.:1414948-59-6
Molecular Formula:C₁₂H₁₄N₂O₆S
Molecular Weight:314.319
Hs Code.:

Synonyms:(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

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Chemical Property of (S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

Chemical Property:

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Technology Process of (S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

There total 3 articles about (S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1414948-57-4
(S)-methyl 2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carboxylate

: 1414948-59-6
(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

Guidance literature:: (S)-methyl 2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carboxylate; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1.5h; Inert atmosphere;

With water; rochelle salt; In methanol; ethyl acetate; toluene; at 20 ℃; for 1h;
DOI:10.1055/s-0032-1316579

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1414948-59-6
(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 16.5 h / 20 °C / Inert atmosphere

2.1: water; toluene-4-sulfonic acid / benzene / 2.5 h / Reflux

3.1: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C / Inert atmosphere

3.2: 1 h / 20 °C

With water; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene; benzene;
DOI:10.1055/s-0032-1316579

Reference yield:

: L-serine methyl ester hydrochloride

: 1414948-59-6
(S)-2,2-dimethyl-3-[(4-nitrophenyl)sulfonyl]oxazolidine-4-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; toluene-4-sulfonic acid / benzene / 2.5 h / Reflux

2.1: diisobutylaluminium hydride / toluene / 1.5 h / -78 °C / Inert atmosphere

2.2: 1 h / 20 °C

With water; diisobutylaluminium hydride; toluene-4-sulfonic acid; In toluene; benzene;
DOI:10.1055/s-0032-1316579