methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside

Base Information

• Chemical Name: methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside
• CAS No.: 135186-64-0
• Molecular Formula: C₃₃H₄₁NO₇
• Molecular Weight: 563.691

Synonyms:methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside

Chemical Property of methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside

There total 11 articles about methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside (1281971-16-1) → methyl 2-[(tert-butoxycarbonyl)amino]-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside (135186-64-0,135186-63-9)

Guidance literature:

With hydrazine hexahydrate; In methanol; at 20 ℃; for 1h;

DOI:10.1002/ejoc.201200522

Reference yield: 73.0%

methyl 3,4,6-tri-O-benzyl-2-C-carbamoyl-2-deoxy-β-D-glucopyranoside (120288-04-2) + tert-butyl alcohol (75-65-0) → methyl 2-[(tert-butoxycarbonyl)amino]-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside (135186-64-0,135186-63-9)

Guidance literature:

With lead(IV) acetate; In N,N-dimethyl-formamide; for 3h; Heating;

DOI:10.1055/s-1991-26443

Reference yield: 69.0%

methyl 3,4,6-tri-O-benzyl-2-C-carbamoyl-2-deoxy-β-D-galactopyranoside (120288-03-1) + tert-butyl alcohol (75-65-0) → methyl 3,4,6-tri-O-benzyl-2-(tert-butoxycarbonyl)amino-2-deoxy-β-D-galactopyranoside (135186-64-0)

Guidance literature:

With lead(IV) acetate; In N,N-dimethyl-formamide; for 3h; Heating;

DOI:10.1055/s-1991-26443

upstream raw materials:

methyl 3,4,6-tri-O-benzyl-2-C-carbamoyl-2-deoxy-β-D-glucopyranoside

tert-butyl alcohol

methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside

methyl N-acetyl-D-glucosamine

Downstream raw materials:

methyl 2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside

methyl 2-methylamino-2-deoxy-3,4,6-tri-O-benzyl-β-D-glucopyranoside

methyl 2-N-methyl-(2-benzyloxy)acetamido-2-deoxy-3,4,6-tri-O-benzyl-β-D-glucopyranoside

methyl 2-N-methyl-(2-benzylcarboxyamino)acetamido-2-deoxy-3,4,6-tri-O-benzyl-β-D-glucopyranoside

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