(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

Base Information

Chemical Name:(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide
CAS No.:189946-12-1
Molecular Formula:C₁₅H₂₄N₂O₅S
Molecular Weight:344.432
Hs Code.:

Synonyms:(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

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Technology Process of (S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

There total 4 articles about (S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 554-52-9
3-Methoxytyramine

: 97482-31-0
(S)-N-(methylsulphonyl)valine

: 189946-12-1
(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
DOI:10.2533/000942903777678542

Reference yield:

: 22568-51-0
(E)-2-methoxy-4-(2-nitrovinyl)phenol

: 189946-12-1
(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄

2: H₂ / Pd/C

3: 71 percent / BOP; iPr₂NEt

With sodium tetrahydroborate; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal;
DOI:10.2533/000942903777678542

Reference yield:

: 528594-30-1
2-methoxy-4-(2-nitroethyl)phenol

: 189946-12-1
(S)-N-[2-(4-hydroxy-3-methoxy-phenyl)-ethyl]-2-methanesulfonylamino-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C

2: 71 percent / BOP; iPr₂NEt

With hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal;
DOI:10.2533/000942903777678542