Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI)

Base Information

• Chemical Name: Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI)
• CAS No.: 528594-30-1
• Molecular Formula: C9H11NO4
• Molecular Weight: 197.191
• Hs Code.: 2909500000
• Mol file: 528594-30-1.mol

Synonyms:Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI)

Chemical Property of Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI)

Chemical Property:

• Melting Point: 160℃
• Boiling Point: 366℃
• Flash Point: 175℃
• PSA: 75.28000
• Density: 1.252
• LogP: 1.74320

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-4-(2-nitroethyl)phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI)

There total 4 articles about Phenol, 2-methoxy-4-(2-nitroethyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(E)-2-methoxy-4-(2-nitrovinyl)phenol (22568-51-0) → 2-methoxy-4-(2-nitroethyl)phenol (528594-30-1)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 - 20 ℃;

DOI:10.1021/acs.orglett.6b01496

Reference yield: 93.1%

(E)-2-methoxy-4-(2-nitrovinyl)phenol (22568-51-0) → C18H20N2O8 + 2-methoxy-4-(2-nitroethyl)phenol (528594-30-1)

Guidance literature:

With sodium tetrahydroborate; ethanol; In water; at 0 ℃; for 2h;

Reference yield: 70.0%

vanillalnitromethane (6178-42-3) → 2-methoxy-4-(2-nitroethyl)phenol (528594-30-1)

Guidance literature:

With borane-ammonia complex; In glycerol; at 60 ℃; for 18h; Green chemistry;

DOI:10.3762/bjoc.17.83

upstream raw materials:

(E)-2-methoxy-4-(2-nitrovinyl)phenol

vanillalnitromethane

vanillin

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