6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

Base Information

Chemical Name:6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one
CAS No.:1184303-37-4
Molecular Formula:C₁₅H₁₃BrN₂O₃
Molecular Weight:349.184
Hs Code.:

Synonyms:6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

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Chemical Property of 6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

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Technology Process of 6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

There total 1 articles about 6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 337463-88-4
6-bromo-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one

: 824-94-2
p-methoxybenzyl chloride

: 1184303-37-4
6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield: 97.0%

: 1184303-37-4
6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

: rel-benzyl (3aR*,7aS*)-2-oxooctahydro-[1,3]oxazolo[5,4-c]pyridine-5-carboxylate

: rel-benzyl (3aR*,7aS*)-1-{4-[(4-methoxyphenyl)methyl]-3-oxo-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-6-yl}-2-oxooctahydro[1,3]oxazolo[5,4-c]pyridine-5-carboxylate

Guidance literature:: With copper(l) iodide; potassium carbonate; trans-1,2-cyclohexanediamine; In 1,4-dioxane; at 0 - 100 ℃; for 24h; Inert atmosphere;

Reference yield: 96.0%

: 4248-19-5
tert-butyl carbazate

: 1184303-37-4
6-bromo-4-[(4-methoxyphenyl)methyl]-2H,3H,4H-pyrido[3,2-b][1,4]oxazin-3-one

: 1619974-79-6
[4-(4-methoxybenzyl)-3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl]carbamic acid tert-butyl ester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 90 ℃; for 96h; Inert atmosphere;