1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine

Base Information

• Chemical Name: 1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine
• CAS No.: 1171245-02-5
• Molecular Formula: C₂₃H₃₂BClN₂O₂
• Molecular Weight: 414.783

Synonyms:1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine

Chemical Property of 1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine

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Technology Process of 1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine

There total 1 articles about 1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N1-(4-bromophenyl)-1-(4-chlorophenyl)-N2-isopropylethane-1,2-diamine (1171245-01-4) + bis(pinacol)diborane (73183-34-3) → 1-(4-chlorophenyl)-N2-isopropyl-N1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine (1171245-02-5)

Guidance literature:

With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dimethyl sulfoxide; at 80 ℃; Inert atmosphere;

Reference yield: 12.0%

(5R,7R)-4-chloro-5-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-7-yl 4-nitrobenzoate (1171244-79-3) + 1-(4-chlorophenyl)-N2-isopropyl-N1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine (1171245-02-5) → (5R,7R)-4-(4-(1-(4-chlorophenyl)-2-(isopropylamino)ethylamino)phenyl)-5-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-7-ol hydrochloride (1171244-56-6)

Guidance literature:

(5R,7R)-4-chloro-5-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-7-yl 4-nitrobenzoate; 1-(4-chlorophenyl)-N₂-isopropyl-N₁-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethane-1,2-diamine; With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In propan-1-ol; water; at 90 ℃; for 14h; Inert atmosphere;

With hydrogenchloride; In dichloromethane;

upstream raw materials:

N₁-(4-bromophenyl)-1-(4-chlorophenyl)-N₂-isopropylethane-1,2-diamine

bis(pinacol)diborane

Downstream raw materials:

(5R,7R)-4-(4-(1-(4-chlorophenyl)-2-(isopropylamino)ethylamino)phenyl)-5-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-7-ol hydrochloride

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