benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside
CAS No.:120596-17-0
Molecular Formula:C₂₉H₃₂FNO₅
Molecular Weight:493.575
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

There total 5 articles about benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120596-16-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(methylsulfonyl)-α-D-glucopyranoside

: 120596-17-0
benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; for 72h; Heating;
DOI:10.1016/0008-6215(90)84293-4

Reference yield: 25.0%

: 55287-49-5
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 120596-17-0
benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 50 ℃; for 2h;
DOI:10.1016/0008-6215(90)84293-4

Reference yield:

: 38416-18-1
benzyl 2-acetamido-3-O-benzyl-2-deoxy-4-O-mesyl-6-O-trityl-α-D-glucopyranoside

: 120596-17-0
benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / aq. acetic acid / 2 h / 90 - 100 °C

2: 87 percent / BaO, Ba(OH)2 / dimethylformamide / Ambient temperature

3: 91 percent / tetrabutylammonium fluoride / acetonitrile / 72 h / Heating

With barium dihydroxide; tetrabutyl ammonium fluoride; acetic acid; barium(II) oxide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(90)84293-4