sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate

Base Information

• Chemical Name: sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate
• CAS No.: 1153619-02-3
• Molecular Formula: C₁₇H₁₇N₄O₃*Na
• Molecular Weight: 348.337
• Mol file: 1153619-02-3.mol

Synonyms:sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate

Chemical Property of sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate

There total 1 articles about sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-Aminohippuric acid (61-78-9) → sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate (1153619-02-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium carbonate / Reflux

1.2: Cooling with ice

2.1: acetic acid

With sodium carbonate; acetic acid;

DOI:10.1016/j.bmc.2013.01.014

Reference yield: 47.0%

p-trifluoromethoxybenzaldehyde (659-28-9) + sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate (1153619-02-3) → 2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-{1-[4-(trifluoromethoxy)phenyl]methylidene}-1,3-oxazol-5-one (1428486-00-3)

Guidance literature:

With sodium acetate; acetic anhydride; at 100 ℃;

DOI:10.1016/j.bmc.2013.01.014

Reference yield: 42.0%

sodium 2-[4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}benzoylamino]acetate (1153619-02-3) + 4-fluorobenzaldehyde (459-57-4) → 2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-[1-(4-fluorophenyl)methylidene]-1,3-oxazol-5-one (1428485-99-7)

Guidance literature:

With sodium acetate; acetic anhydride; at 100 ℃;

DOI:10.1016/j.bmc.2013.01.014

upstream raw materials:

p-Aminohippuric acid

Downstream raw materials:

2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-[1-(4-fluorophenyl)methylidene]-1,3-oxazol-5-one

2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-{1-[4-(trifluoromethoxy)phenyl]methylidene}-1,3-oxazol-5-one