3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

Base Information

Chemical Name:3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone
CAS No.:89448-50-0
Molecular Formula:C₁₂H₁₂O₄
Molecular Weight:220.225
Hs Code.:

Synonyms:3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

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Chemical Property of 3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

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Technology Process of 3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

There total 4 articles about 3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 89448-49-7
3,5-O-Benzylidene-2-O-<(methylthio)thiocarbonyl>-D-ribonic Acid γ-Lactone

: 89448-50-0
3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; Heating;
DOI:10.1016/S0040-4039(00)94032-2

Reference yield:

: 20603-44-5,104445-18-3,131614-82-9,131614-83-0
3,5-O-Benzylidene-D-ribonic Acid γ-Lactone

: 89448-50-0
3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 1. sodium hydride / 1. dimethylformamide, room temperature, 30 min 2. 30 min, room temperature

2: 92.5 percent / tri-n-butyltin hydride, AIBN / toluene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In toluene;
DOI:10.1021/jo00186a018

Reference yield:

: 100-52-7
benzaldehyde

: 89448-50-0
3,5-O-Benzylidene-2-deoxy-D-ribonic Acid γ-Lactone

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / 7 h / Ambient temperature

2: 1. sodium hydride / 1. dimethylformamide, room temperature, 30 min 2. 30 min, room temperature

3: 92.5 percent / tri-n-butyltin hydride, AIBN / toluene / 2 h / Heating

With hydrogenchloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In toluene;
DOI:10.1021/jo00186a018