5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

Base Information

Chemical Name:5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid
CAS No.:1084949-34-7
Molecular Formula:C₂HF₃O₂*C₂₁H₂₂N₆
Molecular Weight:472.47
Hs Code.:

Synonyms:5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

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Chemical Property of 5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

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Technology Process of 5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

There total 6 articles about 5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1295434-59-1
Br^(1-)*C₅₉H₅₁N₆⁽¹⁺⁾

: 76-05-1
trifluoroacetic acid

: 1084949-34-7
5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

Guidance literature:: With triethylsilane; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1007/s10822-010-9371-3

Reference yield:

: 1084949-58-5
3-(triphenylmethyl)-5-butylimidazole

: 1084949-34-7
5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 24 h / 20 °C / Inert atmosphere

2: triethylsilane / dichloromethane / 1 h / 20 °C

With triethylsilane; In dichloromethane;
DOI:10.1007/s10822-010-9371-3

Reference yield:

: 133909-97-4
N-(trityl)-5-[4?-(methyl)biphenyl-2-yl]-2H-tetrazole

: 1084949-34-7
5-butyl-1-[[2'-(2H-tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole trifluoroacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux

2: dichloromethane / 24 h / 20 °C / Inert atmosphere

3: triethylsilane / dichloromethane / 1 h / 20 °C

With triethylsilane; N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; dichloromethane;
DOI:10.1007/s10822-010-9371-3