benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

Base Information

Chemical Name:benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate
CAS No.:1396312-89-2
Molecular Formula:C₃₉H₄₂N₆O₅
Molecular Weight:674.8
Hs Code.:

benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

Synonyms:benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

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Chemical Property of benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

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Technology Process of benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

There total 6 articles about benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: benzyl (S,S)-1-(1-azidopropan-2-ylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

: 1396312-81-4
8-but-3-ynyl-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-10-one

: 1396312-89-2
benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In water; dimethyl sulfoxide; at 80 ℃; for 16h;
DOI:10.1055/s-0031-1291145

Reference yield:

: 100330-50-5
3-oxo-hept-6-ynoic acid methyl ester

: 1396312-89-2
benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triisopropoxytitanium(IV) chloride / toluene / Reflux

1.2: 20 °C

2.1: copper(II) sulfate; sodium L-ascorbate / water; dimethyl sulfoxide / 16 h / 80 °C

With triisopropoxytitanium(IV) chloride; copper(II) sulfate; sodium L-ascorbate; In water; dimethyl sulfoxide; toluene; 1.1: Pechmann condensation / 2.1: Huisgen-Meldal-Shapeles reaction;
DOI:10.1055/s-0031-1291145

Reference yield:

: C₂₁H₂₃F₃N₂O₆S

: 1396312-89-2
benzyl (S,S)-1-(1-methyl-2-{4-[2-(10-oxo-2,3,5,6-tetrahydro-1H,4H-11-oxa-3a-azabenzo[de]anthracen-8-yl)ethyl]-1,2,3-triazol-1-yl}ethylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 16 h / 60 °C

2: copper(II) sulfate; sodium L-ascorbate / water; dimethyl sulfoxide / 16 h / 80 °C

With sodium azide; copper(II) sulfate; sodium L-ascorbate; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Huisgen-Meldal-Shapeles reaction;
DOI:10.1055/s-0031-1291145