methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

Base Information

Chemical Name:methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate
CAS No.:1621518-07-7
Molecular Formula:C₂₇H₄₃NO₄SSi
Molecular Weight:505.794
Hs Code.:

Synonyms:methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

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Chemical Property of methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

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Technology Process of methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

There total 6 articles about methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1626404-73-6
methyl 2-(1-(tert-butyldimethylsilyloxy)-2-(4-octylphenoxy)ethyl)-4,5-dihydrothiazole-4-carboxylate

: 1621518-07-7
methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

Guidance literature:: With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃;

Reference yield:

: 1621517-96-1
2-(tert-butyldimethylsilyloxy)-3-(4-octylphenoxy)propanenitrile

: 1621518-07-7
methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / methanol / 20 °C

2: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

With Bromotrichloromethane; ammonium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane;

Reference yield:

: 51437-89-9
2-(4-octylphenoxy)ethanol

: 1621518-07-7
methyl 2-(1-((tert-butyldimethylsilyl)oxy)-2-(4-octylphenoxy)ethyl)thiazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bromide; sodium hypochlorite; sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / toluene; ethyl acetate; water / -5 °C

1.2: 20 °C / Inert atmosphere

2.1: ammonium acetate / methanol / 20 °C

3.1: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; Bromotrichloromethane; ammonium acetate; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium bromide; In methanol; dichloromethane; water; ethyl acetate; toluene;