N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide)

Base Information

Chemical Name:N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide)
CAS No.:27998-17-0
Molecular Formula:C18H20 N2 S2
Molecular Weight:328.4948
Hs Code.:
NSC Number:231414
DSSTox Substance ID:DTXSID00394658
Mol file:27998-17-0.mol

Synonyms:27998-17-0;NSC231414;N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide);DTXSID00394658;NSC-231414

Suppliers and Price of N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide)

Chemical Property:

Boiling Point:477.9°Cat760mmHg
Flash Point:242.8°C
Density:1.187g/cm³
XLogP3:4.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:328.10679099
Heavy Atom Count:22
Complexity:311

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCNC(=S)C(=S)NCCC2=CC=CC=C2

Technology Process of N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide)

There total 2 articles about N~1~,N~2~-Bis(2-phenylethyl)ethanebis(thioamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 107-14-2
chloroacetonitrile

: 64-04-0
phenethylamine

: 27998-17-0
bis(β-phenylethyl)dithiooxamide

Guidance literature:: With sulfur; In N,N-dimethyl-formamide; at 70 ℃; for 8h;

Reference yield: 24.0%

: 17008-22-9
methyl cyanodithioformate

: 64-04-0
phenethylamine

: 27998-17-0
bis(β-phenylethyl)dithiooxamide

Guidance literature:: In ethanol; for 16h; Ambient temperature;

Reference yield: 83.0%

: 75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9
cis-dichlorobis(dimethylsulfoxide)platinum(II)

: 27998-17-0
bis(β-phenylethyl)dithiooxamide

: 1192736-14-3
[(bis(β-phenylethyl)dithiooxamidato)Pt(bis(β-phenylethyl)dithiooxamide)]Cl

Guidance literature:: With NaHCO₃; In CHCl₃; byproducts: HCl, (CH3)2SO; Pt complex suspended in CHCl3 together with NaHCO3, ligand added, allowed to stand for 1 h, filtered, ligand added, allowed to stand for 1 h; concd., pptd. (petroleum ether); elem. anal.;
DOI:10.1021/ic900875b