di-o-tolyl((trimethylsilyl)ethynyl)phosphane

Base Information

Chemical Name:di-o-tolyl((trimethylsilyl)ethynyl)phosphane
CAS No.:1613321-99-5
Molecular Formula:C₁₉H₂₃PSi
Molecular Weight:310.451
Hs Code.:

Synonyms:di-o-tolyl((trimethylsilyl)ethynyl)phosphane

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Chemical Property of di-o-tolyl((trimethylsilyl)ethynyl)phosphane

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Technology Process of di-o-tolyl((trimethylsilyl)ethynyl)phosphane

There total 1 articles about di-o-tolyl((trimethylsilyl)ethynyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 36042-94-1
bis(o-tolyl)chlorophosphine

: 1066-54-2
trimethylsilylacetylene

: 1613321-99-5
di-o-tolyl((trimethylsilyl)ethynyl)phosphane

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.5h;

bis(o-tolyl)chlorophosphine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja5028293

Reference yield: 81.0%

: 1003010-55-6
Ph₂P-C₂H₄-B(C₆F₅)2

: 1613321-99-5
di-o-tolyl((trimethylsilyl)ethynyl)phosphane

: 1613321-84-8
C₅₁H₄₉BF₁₀P₂Si

Guidance literature:: In toluene; at 70 ℃; Inert atmosphere;
DOI:10.1021/ja5028293

Reference yield:

: 1613321-99-5
di-o-tolyl((trimethylsilyl)ethynyl)phosphane

: C₅₁H₆₀BNO₂P₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 70 °C / Inert atmosphere

2: benzene / 20 °C / 1125.11 Torr / Inert atmosphere

3: cyclohexa-1,4-diene / toluene / 20 °C / Inert atmosphere

With cyclohexa-1,4-diene; In toluene; benzene;
DOI:10.1021/ja5028293