Technology Process of 8-(4-methoxy-2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)octyl nitrate
There total 6 articles about 8-(4-methoxy-2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)octyl nitrate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium peroxodisulfate; silver nitrate;
In
water; acetonitrile;
at 75 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide; trichloroisocyanuric acid / acetone / 3.5 h / 0 - 20 °C
2: silver nitrate / acetonitrile / 0.37 h / 120 °C / Microwave irradiation
3: silver nitrate; dipotassium peroxodisulfate / acetonitrile; water / 3 h / 75 °C
With
dipotassium peroxodisulfate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; sodium hydrogencarbonate; silver nitrate; sodium bromide;
In
water; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: [bis(acetoxy)iodo]benzene
2: silver nitrate; dipotassium peroxodisulfate / acetonitrile; water / 3 h / 75 °C
With
dipotassium peroxodisulfate; [bis(acetoxy)iodo]benzene; silver nitrate;
In
water; acetonitrile;
