methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

Base Information

Chemical Name:methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate
CAS No.:1251548-16-9
Molecular Formula:C₃₀H₂₇ClN₂O₄S
Molecular Weight:547.074
Hs Code.:

Synonyms:methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

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Chemical Property of methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

Chemical Property:

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Technology Process of methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

There total 2 articles about methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 169829-11-2
N-(m-chlorobenzylidene)-4-methylbenzenesulfonamide

: 1073118-19-0
(anti)-methyl 3-(m-chlorophenyl)-2-[(diphenylmethylene)amino]-3-(p-toluenesulfonylamino)propanoate

: 1251548-16-9
methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

: methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

: (syn)-methyl 3-(m-chlorophenyl)-2-[(diphenylmethylene)amino]-3-(p-toluenesulfonylamino)propanoate

Guidance literature:: With silver trifluoromethanesulfonate; (3,5-Dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-((R)-1-phenyl-ethyl)-amine; In toluene; at 20 ℃; for 24h; Overall yield = 42 %; Overall yield = 27.6 mg; enantioselective reaction;
DOI:10.1016/j.tetasy.2014.11.009

Reference yield:

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 169829-11-2
N-(m-chlorobenzylidene)-4-methylbenzenesulfonamide

: 1251548-16-9
methyl 2-[(diphenylmethylene)amino]-3-(4-methylphenylsulfonamide)-3-(m-chlorophenyl)propanoate

: C₃₀H₂₇ClN₂O₄S

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; (S)-TF-BiphamPhos; BH₄^(1-)*C₈H₁₂CuN₄⁽¹⁺⁾; In dichloromethane; at -30 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000252