N-Cyclohexyl-3-propiolamid

Base Information

• Chemical Name: N-Cyclohexyl-3-propiolamid
• CAS No.: 80048-08-4
• Molecular Formula: C₁₆H₂₀N₂O
• Molecular Weight: 256.348

Synonyms:N-Cyclohexyl-3-propiolamid

Chemical Property of N-Cyclohexyl-3-propiolamid

Chemical Property:

Purity/Quality:

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Technology Process of N-Cyclohexyl-3-propiolamid

There total 2 articles about N-Cyclohexyl-3-propiolamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methyl-N-(trichlorovinyl)aniline (708-88-3) + Cyclohexyl isocyanate (3173-53-3) → N-Cyclohexyl-3-propiolamid (80048-08-4)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) hexane/ether, 2 h, room temp., 2.) 5 h, room temp.;

Reference yield:

N-Methyl-N-(trimethylstannylethinyl)anilin (67370-99-4) + Cyclohexyl isocyanate (3173-53-3) → N-Cyclohexyl-3-propiolamid (80048-08-4)

Guidance literature:

With water; Yield given. Multistep reaction; 1.) ether, room temp., 2.) chloroform/ether;

Reference yield: 86.0%

N-Cyclohexyl-3-propiolamid (80048-08-4) → N-Cyclohexyl-2-(N-methyl-N-phenylthiocarbamoyl)acetamid (99601-06-6)

Guidance literature:

With hydrogen sulfide; In chloroform; for 48h; Ambient temperature;

upstream raw materials:

N-methyl-N-(trichlorovinyl)aniline

Cyclohexyl isocyanate

N-Methyl-N-(trimethylstannylethinyl)anilin

Downstream raw materials:

N-Cyclohexyl-5-(methylphenylamino)-3-phenyl-isoxazolcarboxamid

N'-Cyclohexyl-N-methyl-N-phenyl-propandiamid

N-Cyclohexyl-2-(N-methyl-N-phenylthiocarbamoyl)acetamid

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