4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

Base Information

Chemical Name:4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide
CAS No.:1421922-34-0
Molecular Formula:C₂₃H₂₇N₃OS
Molecular Weight:393.553
Hs Code.:

Synonyms:4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

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Chemical Property of 4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

Chemical Property:

Purity/Quality:

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Technology Process of 4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

There total 6 articles about 4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-33-9
N-tert-butyl-4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzamide

: 1421922-34-0
4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 20h;

Reference yield:

: 1421922-32-8
4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoic acid

: 1421922-34-0
4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 32 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1421922-04-4
2-(2,5-dimethyl-4-nitrophenyl)ethanethioamide

: 1421922-34-0
4-[2-(4-amino-2,5-dimethylbenzyl)-1,3-thiazol-4-yl]-N-tert-butylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: isopropyl alcohol / 2 h / 80 °C

2: sodium hydroxide; water / methanol / 2 h / 50 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 32 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C

With palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide; isopropyl alcohol;