methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

Base Information

Chemical Name:methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide
CAS No.:1421922-30-6
Molecular Formula:BrH*C₂₀H₁₈N₂O₄S
Molecular Weight:463.352
Hs Code.:

Synonyms:methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

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Chemical Property of methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

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Technology Process of methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

There total 3 articles about methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-04-4
2-(2,5-dimethyl-4-nitrophenyl)ethanethioamide

: 56893-25-5
methyl 4-(2-bromoacetyl)benzoate

: 1421922-30-6
methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

Guidance literature:: In isopropyl alcohol; at 80 ℃;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421922-30-6
methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / 0.5 h / Cooling with ice

2: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3: isopropyl alcohol / 2 h / 80 °C

With hydrogenchloride; nitric acid; O,O-Diethyl hydrogen phosphorodithioate; In ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421922-30-6
methyl 4-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]benzoate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2: isopropyl alcohol / 2 h / 80 °C

With hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate; In ethyl acetate; isopropyl alcohol;