5-phenyl-1,3-dehydroadamantane

Base Information

Chemical Name:5-phenyl-1,3-dehydroadamantane
CAS No.:1428321-21-4
Molecular Formula:C₁₆H₁₈
Molecular Weight:210.319
Hs Code.:

Synonyms:5-phenyl-1,3-dehydroadamantane

Suppliers and Price of 5-phenyl-1,3-dehydroadamantane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-phenyl-1,3-dehydroadamantane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-phenyl-1,3-dehydroadamantane

There total 5 articles about 5-phenyl-1,3-dehydroadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 202055-88-7
1,3-dibromo-5-phenyladamantane

: 1428321-21-4
5-phenyl-1,3-dehydroadamantane

Guidance literature:: With lithium; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.042

Reference yield:

: 768-95-6
1-adamanthanol

: 1428321-21-4
5-phenyl-1,3-dehydroadamantane

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 24 h / 50 °C / Inert atmosphere

1.2: 25 h / 0 - 50 °C / Inert atmosphere

2.1: bromine / tetrachloromethane / 12 h / 20 °C

3.1: magnesium; ethylene dibromide / dichloromethane / Inert atmosphere; Reflux

4.1: carbon tetrabromide; tetrabutylammomium bromide; sodium hydroxide / water; fluorobenzene / 48 h / 40 °C

5.1: lithium / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With carbon tetrabromide; tetrabutylammomium bromide; bromine; lithium; sodium hydride; magnesium; ethylene dibromide; sodium hydroxide; In tetrahydrofuran; tetrachloromethane; fluorobenzene; dichloromethane; water; N,N-dimethyl-formamide; 5.1: |Wurtz Reaction;
DOI:10.1016/j.tet.2013.02.042

Reference yield:

: 780-68-7
1-phenyladamantane

: 1428321-21-4
5-phenyl-1,3-dehydroadamantane

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; tetrabutylammomium bromide; sodium hydroxide / water; fluorobenzene / 48 h / 40 °C

2: lithium / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With carbon tetrabromide; tetrabutylammomium bromide; lithium; sodium hydroxide; In tetrahydrofuran; fluorobenzene; water; 2: |Wurtz Reaction;
DOI:10.1016/j.tet.2013.02.042