1,3-dibromo-5-phenyladamantane

Base Information

Chemical Name:1,3-dibromo-5-phenyladamantane
CAS No.:202055-88-7
Molecular Formula:C₁₆H₁₈Br₂
Molecular Weight:370.127
Hs Code.:

Synonyms:1,3-dibromo-5-phenyladamantane

Suppliers and Price of 1,3-dibromo-5-phenyladamantane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dibromo-5-phenyladamantane

Chemical Property:

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Technology Process of 1,3-dibromo-5-phenyladamantane

There total 5 articles about 1,3-dibromo-5-phenyladamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 780-68-7
1-phenyladamantane

: 202055-88-7
1,3-dibromo-5-phenyladamantane

Guidance literature:: With carbon tetrabromide; tetrabutylammomium bromide; sodium hydroxide; In fluorobenzene; water; at 40 ℃; for 48h; Solvent;
DOI:10.1016/j.tet.2013.02.042

Reference yield:

: 768-95-6
1-adamanthanol

: 202055-88-7
1,3-dibromo-5-phenyladamantane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 24 h / 50 °C / Inert atmosphere

1.2: 25 h / 0 - 50 °C / Inert atmosphere

2.1: bromine / tetrachloromethane / 12 h / 20 °C

3.1: magnesium; ethylene dibromide / dichloromethane / Inert atmosphere; Reflux

4.1: carbon tetrabromide; tetrabutylammomium bromide; sodium hydroxide / water; fluorobenzene / 48 h / 40 °C

With carbon tetrabromide; tetrabutylammomium bromide; bromine; sodium hydride; magnesium; ethylene dibromide; sodium hydroxide; In tetrachloromethane; fluorobenzene; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2013.02.042

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 202055-88-7
1,3-dibromo-5-phenyladamantane

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium; ethylene dibromide / dichloromethane / Inert atmosphere; Reflux

2: carbon tetrabromide; tetrabutylammomium bromide; sodium hydroxide / water; fluorobenzene / 48 h / 40 °C

With carbon tetrabromide; tetrabutylammomium bromide; magnesium; ethylene dibromide; sodium hydroxide; In fluorobenzene; dichloromethane; water;
DOI:10.1016/j.tet.2013.02.042