6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

Base Information

Chemical Name:6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose
CAS No.:1253692-53-3
Molecular Formula:C₇₇H₈₂O₁₁Si
Molecular Weight:1211.58
Hs Code.:

Synonyms:6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

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Chemical Property of 6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

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Technology Process of 6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

There total 3 articles about 6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-20-7
TREHALOSE

: 100-39-0
benzyl bromide

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1253692-53-3
6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

: 1253692-54-4
6,6'-di-O-tert-butyldiphenylsilyl-2,3,4,2',3',4'-hexa-O-benzyl-α,α-D-trehalose

Guidance literature:: TREHALOSE; tert-butylchlorodiphenylsilane; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 36h;

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1253891-15-4
6-O-tert-butyldiphenylsilyl-D-trehalose

: 100-39-0
benzyl bromide

: 1253692-53-3
6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 24h; Inert atmosphere;

Reference yield:

: 99-20-7
TREHALOSE

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1253692-53-3
6-O-tert-butyldiphenylsilyl-2,3,4,2',3',4',6'-hepta-O-benzyl-α,α-D-trehalose

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 24 h / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/ja204249p