8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE

Base Information

Chemical Name:8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE
CAS No.:98408-17-4
Molecular Formula:C₁₀H₁₂BrClN₄O₂
Molecular Weight:335.588
Hs Code.:
Mol file:98408-17-4.mol

Synonyms:8-bromo-7-(3-chloropropyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione

Suppliers and Price of 8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE 95.00%
5MG
$ 497.29

Total 3 raw suppliers

Chemical Property of 8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE

Chemical Property:

Purity/Quality:: 8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE

There total 7 articles about 8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 10381-75-6
8-bromotheophylline

: 109-70-6
1.3-chlorobromopropane

: 98408-17-4
8-bromo-7-(3-chloropropyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone; for 10h; Heating;
DOI:10.1515/znb-2001-0317

Reference yield: 85.0%

: 142-28-9
1,3-Dichloropropane

: 10381-75-6
Bromotheophylline

: 98408-17-4
8-bromo-7-(3-chloropropyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; for 2h; Heating;

Reference yield:

: 58-55-9,75448-53-2
theophylline

: 98408-17-4
8-bromo-7-(3-chloropropyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorate; hydrogen bromide; acetic acid

2: N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate / acetone

With sodium chlorate; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; potassium carbonate; acetic acid; In acetone;
DOI:10.1016/j.ejmech.2011.05.023