trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Base Information

Chemical Name:trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)
CAS No.:147264-58-2
Molecular Formula:C₃₄H₃₄Cl₂O₆P₂Ru
Molecular Weight:772.564
Hs Code.:

Synonyms:trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Suppliers and Price of trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

There total 1 articles about trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 147264-53-7
trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

: 147264-58-2
trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Guidance literature:: With carbon monoxide; In dichloromethane; under Ar, bubbling CO through a soln. of Ru-compd. at room temp. until the red soln. turned light yellow; evapn. to low volume, pptn. upon addn. of n-hexane with stirring, filtration, washing (n-hexane), drying in vac., elem. anal.;

Reference yield: 72.0%

: 147264-58-2
trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

: 147244-85-7
trans-dichloro-cis-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

: 147264-62-8
carbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P;O',P'}ruthenium(II)

Guidance literature:: In dichloromethane; under Ar, dropwise addn. of trans-dichloro-cis-bis((1,3-dioxolane-4-ylmethyl)diphenylphosphine-O,P)ruthenium(II) to trans-dicarbonyl-trans-dichloro-trans-bis((1,3-dioxolane-4-ylmethyl)diphenylphosphine-P)ruthenium(II), stirring for 30 min at room temp.; evapn. to low volume, pptn. upon addn. of n-hexane, washing (n-hexane), drying in vac., elem. anal.;