trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

Base Information

Chemical Name:trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)
CAS No.:147264-53-7
Molecular Formula:C₃₂H₃₄Cl₂O₄P₂Ru
Molecular Weight:716.543
Hs Code.:

Synonyms:trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

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Chemical Property of trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

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Technology Process of trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

There total 1 articles about trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 73785-74-7
(diphenylphosphino)acetaldehyde ethylene acetal

: 147264-53-7
trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

Guidance literature:: In dichloromethane; under Ar, addn. of (1,3-dioxolane-2-ylmethyl)diphenylphosphine soln. to a stirred soln. of RuCl2(PPh3)3, stirring for 30 min at room temp.; evapn., extg. (n-hexane), filtration, washing (n-hexane), drying in vac., elem. anal.;

Reference yield: 65.0%

: 147264-53-7
trans-dichloro-cis-bis{(1,3-dioxolane-2-ylmethyl)diphenylphosphine-O,P}ruthenium(II)

: 147264-58-2
trans-dicarbonyl-trans-dichloro-trans-bis{(1,3-dioxolane-4-ylmethyl)diphenylphosphine-P}ruthenium(II)

Guidance literature:: With carbon monoxide; In dichloromethane; under Ar, bubbling CO through a soln. of Ru-compd. at room temp. until the red soln. turned light yellow; evapn. to low volume, pptn. upon addn. of n-hexane with stirring, filtration, washing (n-hexane), drying in vac., elem. anal.;